MOLECULAR AND CRYSTAL STRUCTURES OF 3-[(4-METOXIDIPHENYL)DIAZENIL]PENTANE-2,4-DION

Kh.J.Nagiyev, A.Y.Abiyeva, R.A.Aliyeva, R.K.Askerov, F.M.Chiragov

A new β-diketone on the base of acetilacetone – 3-[(4-metoxidiphenyl)diazenyl]pentane-2,4-dion has been synthesized. Its molecular and crystal structure was solved by using of X-ray difraction methods. The crystals are monoclinic: a=8.019 (6), b=6.379(4), c=10.941(8) Å, β=94.430 (13)⁰, V=557.9(7) Å³, space group P2₁/m, Z=2, density (calculated) 1.394 g/cm³, absorption coefficient 0.102 mm^-1, crystal size 0.20×0.30×0.27 mm³. It`s been found out, that synthesized compound belongs to hydrazo-form.

Keywords : 3-[(4-metoxidiphenyl) diazenil]pentane-2,4-dion, X-ray analysis, crystal structure

View article

SUBMITION

THE LAST NUMBER OF THE JOURNAL

№1 2023

CONTENT

- PLATINUM – MESOPOROUS CARBON NITRIDE NANOCOMPOSITES: SYNTHESIS, CHARACTERIZATION AND CATALYTIC PERFORMANCE IN PHENYLACETYLENE HYDROGENATIONV.M.Akhmedov, N.E.Melnikova, G.G.Nurullayev, Vs.M.Ahmadov, D.B.Tagiyev

- Ag8GeS6(Se6)–Ag8GeTe6 SYSTEMS: PHASE RELATIONS, SYNTHESIS, AND CHARACTERIZATION OF SOLID SOLUTIONSA.J.Amiraslanova, A.T.Mammadova, I.J.Alverdiyev, Yu.A.Yusibov, M.B.BabanlyMore