DETERMINATION OF PRIMARY CRYSTALLIZATION REGION OF THE CHALCOPYRITE PHASE IN THE CuInSe2-Pb-Se SYSTEM
Interaction in the CuInSe2-Pb-Se quasi ternary system were studied by DTA, X-ray powder diffraction, microstructural analysis and microhardnes measurements. A projection of the liquidus surface of the phase diagram was constructed, where the boundaries of the primary crystallization region of the low-temperature chalcopyrite phase were determined. The existence of the compound with a rational formula CuInPbSe2 was established, which forms at 6500C by a peritectic reaction
Keywords : system CuInSe2-Pb-Se, primary crystallization region, solidus, eutectic, peritectic
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