ISSN 0005-2531 (Print) ISSN 2522-1841 (Online)
MICROWAVE RADIATION STIMULATED REACTION OF ACYLATION OF DIETHYL-AMINE WITH M-TOLUIC ACID IN THE PRESENCE OF Zn-B-P/Al2O3/Al CATALYST
P.A.Muradova

The paper presents the results of microwave synthesis of a Zn-B-P-oxide catalyst, which actively absorbs the energy of microwave radiation, applied to the surface of an aluminum-reinforced Al/γ-Al2O3 carrier, in order to further intensify the process of acylation of diethylamine with m-toluic acid to diethylamide m-toluic acid (DETA) under conditions of exposure to a microwave field. The results obtained demonstrate the possibility of realizing the process of acylation of diethylamine with m-toluic acid in a thermal regime, which is formed in the reaction zone due to the transformation of microwave energy by the catalyst mass. The developed method of microwave acylation of diethylamine with m-toluic acid is superior to the existing analogs in technological and energy parameters.

 doi.org/10.32737/0005-2531-2022-3-110-116

Keywords : microwave radiation, m-toluic acid, diethylamine, acylation, dietylamide of m-toluic acid
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№2 2024
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